ICS67.140.20CCSX51CASME標(biāo)準(zhǔn)Generaltechnicalrequirementsforfreeze-driedcoffee中國(guó)中小商業(yè)企業(yè)協(xié)會(huì)發(fā)布IT/CASME1712-2024本文件按照GB/T1.1—2020《標(biāo)準(zhǔn)化工作導(dǎo)則第1部分：標(biāo)準(zhǔn)化文件的結(jié)構(gòu)和起草規(guī)則》的規(guī)定起請(qǐng)注意本文件的某些內(nèi)容可能涉及專利。本文件的發(fā)布機(jī)構(gòu)不承擔(dān)識(shí)別專利的責(zé)任。本文件由北京正能量美能生物科技有限公司提出。本文件由中國(guó)中小企業(yè)商業(yè)協(xié)會(huì)歸口。本文件起草單位：北京正能量美能生物科技有限公司、中檢科（上海）測(cè)試技術(shù)有限公司、中國(guó)農(nóng)業(yè)大學(xué)食品科學(xué)與營(yíng)養(yǎng)工程學(xué)院、中國(guó)綠色食品有限公司、中國(guó)檢驗(yàn)認(rèn)證集團(tuán)上海有限公司、首都保健營(yíng)養(yǎng)美食學(xué)會(huì)、北京工商大學(xué)食品與健康學(xué)院、天益食品（徐州）有限公司、天利食品科技有限公司、上海投創(chuàng)網(wǎng)絡(luò)科技有限公司、山東農(nóng)業(yè)工程學(xué)院、塔里木大學(xué)食品科學(xué)與工程學(xué)院、吉林外國(guó)語(yǔ)大學(xué)。本文件主要起草人：楊浩、樂粉鵬、王旭峰、王倩、周峰、趙亮、丁朋、楊志偉、游環(huán)、魏陽(yáng)吉、潘志明、褚芳芳、遲曉君、邢吉樂、郭東起、高原、鄭極慶、付文鈺。本文件首次發(fā)布。T/CASME1712-2024版權(quán)聲明本文件由中國(guó)中小商業(yè)企業(yè)協(xié)會(huì)（簡(jiǎn)稱“協(xié)會(huì)”）組織創(chuàng)制的團(tuán)體標(biāo)準(zhǔn)文本（含制定過程中的草案協(xié)會(huì)擁有本文件的著作權(quán)，受《中華人民共和國(guó)著作權(quán)法》保護(hù)。除法律所允許的情形或事先得到協(xié)會(huì)書面許可外，任何組織和個(gè)人不得以任何理由進(jìn)行復(fù)制、銷售、傳播本文件，或抄襲、歪曲本文件等侵權(quán)行為：否則行為人應(yīng)承擔(dān)相應(yīng)的民事、行政責(zé)任，構(gòu)成犯罪的，將依法追究其刑事責(zé)任。其他文件引用本文件，不屬侵權(quán)行為，標(biāo)準(zhǔn)聯(lián)合起草單位可以使用本標(biāo)準(zhǔn)。凡利用本文件進(jìn)行或支持貿(mào)易、認(rèn)證等商業(yè)活動(dòng)，應(yīng)事先購(gòu)買正式文本或得到協(xié)會(huì)書面授權(quán)。購(gòu)買本文件或獲得授權(quán)，請(qǐng)與協(xié)會(huì)聯(lián)系。歡迎社會(huì)各界舉報(bào)侵權(quán)盜版行為，協(xié)會(huì)將依法嚴(yán)格保護(hù)舉報(bào)人信息。聯(lián)系電話系郵箱：107073022@協(xié)會(huì)對(duì)本版權(quán)聲明擁有最終解釋權(quán)。T/CASME1712-2024凍干咖啡通用技術(shù)要求本文件規(guī)定了凍干咖啡的術(shù)語(yǔ)和定義、技術(shù)要求、檢驗(yàn)規(guī)則、標(biāo)志標(biāo)簽、包裝、運(yùn)輸、貯存、保質(zhì)期。本文件適用于凍干咖啡的生產(chǎn)、檢驗(yàn)和銷售。2規(guī)范性引用文件下列文件中的內(nèi)容通過文中的規(guī)范性引用而構(gòu)成本文件必不可少的條款。其中，注日期的引用文件，僅該日期對(duì)應(yīng)的版本適用于本文件；不注日期的引用文件，其最新版本（包括所有的修改單）適用于本文件。GB2760食品安全國(guó)家標(biāo)準(zhǔn)食品添加劑使用標(biāo)準(zhǔn)GB2761食品安全國(guó)家標(biāo)準(zhǔn)食品中真菌毒素限量GB2762食品安全國(guó)家標(biāo)準(zhǔn)食品中污染物限量GB5009.3食品安全國(guó)家標(biāo)準(zhǔn)食品中水分的測(cè)定GB5009.5食品安全國(guó)家標(biāo)準(zhǔn)食品中蛋白質(zhì)的測(cè)定GB5009.11食品安全國(guó)家標(biāo)準(zhǔn)食品中總砷及無機(jī)砷的測(cè)定GB5009.12食品安全國(guó)家標(biāo)準(zhǔn)食品中鉛的測(cè)定GB5009.15食品安全國(guó)家標(biāo)準(zhǔn)食品中鎘的測(cè)定GB/T5009.19—2008食品中有機(jī)氯農(nóng)藥多組分殘留量的測(cè)定GB5009.22食品安全國(guó)家標(biāo)準(zhǔn)食品中黃曲霉毒素B族和G族的測(cè)定GB5009.96—2016食品安全國(guó)家標(biāo)準(zhǔn)食品中赭曲霉毒素A的測(cè)定GB5009.139食品安全國(guó)家標(biāo)準(zhǔn)飲料中咖啡因的測(cè)定GB5413.29食品安全國(guó)家標(biāo)準(zhǔn)嬰幼兒食品和乳品溶解性的測(cè)定GB5749生活飲用水衛(wèi)生標(biāo)準(zhǔn)GB7101食品安全國(guó)家標(biāo)準(zhǔn)飲料GB23200.121食品安全國(guó)家標(biāo)準(zhǔn)植物源性食品中331種農(nóng)藥及其代謝物殘留量的測(cè)定液相色譜―質(zhì)譜聯(lián)用法GB7718—2011食品安全國(guó)家標(biāo)準(zhǔn)預(yù)包裝食品標(biāo)簽通則GB/T23379—2009水果、蔬菜及茶葉中吡蟲啉殘留的測(cè)定高效液相色譜法GB28050—2011食品安全國(guó)家標(biāo)準(zhǔn)預(yù)包裝食品營(yíng)養(yǎng)標(biāo)簽通則NY/T604生咖啡NY/T761—2008蔬菜和水果中有機(jī)磷、有機(jī)氯、擬除蟲菊酯和氨基甲酸酯類農(nóng)藥多殘留的測(cè)定NY/T1680蔬菜水果中多菌靈等4種苯并咪唑類農(nóng)藥殘留量的測(cè)定高效液相色譜法SN/T0519—2010進(jìn)出口食品中丙環(huán)唑殘留量的檢測(cè)方法3術(shù)語(yǔ)和定義下列術(shù)語(yǔ)和定義適用于本文件。2T/CASME1712-20243.1凍干咖啡f(wàn)reeze-driedcoffee以咖啡豆或咖啡制品（研磨咖啡粉、咖啡的提取液或其濃縮液等）為主要原料，不添加其他食品原輔料和食品添加劑，經(jīng)冷凍干燥而制取的不規(guī)則晶體塊（粒）狀速溶咖啡。3.2調(diào)制凍干咖啡modulatefreeze-driedcoffee通過添加相關(guān)食品原輔料或添加劑調(diào)制成的凍干咖啡。4技術(shù)要求4.1原輔料要求4.1.1生咖啡豆：應(yīng)符合NY/T604的規(guī)定。4.1.2生產(chǎn)加工用水：應(yīng)符合GB5749的規(guī)定。4.1.3其他原輔料：應(yīng)符合相應(yīng)的標(biāo)準(zhǔn)及有關(guān)規(guī)定，不得使用非食品原料和輔料。4.2要求4.2.1感官要求應(yīng)符合表1的規(guī)定。表1感官要求取適量樣品置于潔凈的白色瓷盤中，在自然光線下觀察產(chǎn)品色澤和狀態(tài)；按標(biāo)簽標(biāo)示的沖調(diào)方法制備樣品，倒入無色透明的容器中，在自然光線下觀察色澤，鑒別氣味，用溫開水漱口品嘗滋味，檢查其有無4.2.2特征性指標(biāo)未沖調(diào)（沖泡）稀釋的固體凍干咖啡產(chǎn)品應(yīng)符合表2的要求。表2特征性指標(biāo)按標(biāo)簽標(biāo)識(shí)的沖調(diào)（沖泡）比例或方法稀釋后產(chǎn)品應(yīng)符合表3的要求。表3特征性指標(biāo)4.2.3理化指標(biāo)應(yīng)符合表4的規(guī)定。3T/CASME1712-2024表4理化指標(biāo)4.3微生物限量應(yīng)符合GB7101的規(guī)定。4.4污染物限量應(yīng)符合GB2762中固體飲料的規(guī)定。4.5真菌毒素限量應(yīng)符合GB2761中固體飲料的規(guī)定。4.6食品添加劑4.6.1純凍干咖啡不應(yīng)添加食品添加劑。4.6.2調(diào)制凍干咖啡食品添加劑質(zhì)量應(yīng)符合相應(yīng)的食品安全標(biāo)準(zhǔn)和有關(guān)規(guī)定，食品添加劑的使用應(yīng)符合GB2760的規(guī)定。5檢驗(yàn)規(guī)則5.1組批以同一次投料加工、同一產(chǎn)品類型、同一班次、同一包裝規(guī)格的產(chǎn)品為一批。5.2取樣從同一批次產(chǎn)品中隨機(jī)抽取，隨機(jī)抽取6個(gè)包裝，樣品分為2份，1份供檢驗(yàn)用，1份備用。5.3檢驗(yàn)5.3.1出廠檢驗(yàn)每批產(chǎn)品均應(yīng)做出廠檢驗(yàn)，經(jīng)檢驗(yàn)合格方可出廠。出廠檢驗(yàn)項(xiàng)目為感官、水分、菌落總數(shù)、大腸桿菌、溶解度、凈含量。5.3.2型式檢驗(yàn)正常情況下，每年進(jìn)行一次，型式檢驗(yàn)項(xiàng)目為本標(biāo)準(zhǔn)規(guī)定的所有項(xiàng)目，發(fā)生以下情況之一時(shí)，亦應(yīng)進(jìn)行檢驗(yàn)：a)產(chǎn)品原料、配方和生產(chǎn)工藝有較大改變時(shí)；b)停產(chǎn)半年以上，重新恢復(fù)生產(chǎn)時(shí)；c)出廠檢驗(yàn)結(jié)果與上一次型式檢驗(yàn)結(jié)果有較大差異時(shí)；d)國(guó)家監(jiān)督管理部門提出此要求時(shí)。5.4判定規(guī)則5.4.1檢驗(yàn)結(jié)果全部項(xiàng)目符合本標(biāo)準(zhǔn)規(guī)定時(shí)，判該批產(chǎn)品為合格品。4T/CASME1712-20245.4.2微生物指標(biāo)中有一項(xiàng)檢驗(yàn)結(jié)果不符合本標(biāo)準(zhǔn)要求時(shí)，判該批產(chǎn)品為不合格品。5.4.3除微生物指標(biāo)外，其他項(xiàng)目檢驗(yàn)結(jié)果不符合本標(biāo)準(zhǔn)要求時(shí)，可以在原批次產(chǎn)品中雙倍抽樣復(fù)驗(yàn)一次，判定以復(fù)驗(yàn)結(jié)果為準(zhǔn)，若有一項(xiàng)指標(biāo)不合格，則判該批產(chǎn)品為不合格品。6標(biāo)志標(biāo)簽、包裝、運(yùn)輸和貯存6.1標(biāo)志標(biāo)簽6.1.1銷售包裝的食品標(biāo)簽標(biāo)識(shí)應(yīng)符合GB7718—2011和GB28050—2011的規(guī)定。6.1.2符合本文件的咖啡產(chǎn)品可以標(biāo)志“凍干咖啡”，符合本文件附錄A的咖啡產(chǎn)品，經(jīng)認(rèn)證可以標(biāo)志“高品質(zhì)凍干咖啡”，并可使用如圖1標(biāo)識(shí)。圖1凍干咖啡認(rèn)證標(biāo)識(shí)6.2包裝包裝材料和容器應(yīng)符合相應(yīng)的食品安全標(biāo)準(zhǔn)及有關(guān)規(guī)定，封口應(yīng)嚴(yán)密、包裝牢固。6.3運(yùn)輸、貯存產(chǎn)品在運(yùn)輸過程中應(yīng)避免日曬、雨淋、重壓；產(chǎn)品應(yīng)在清潔、避光、干燥、通風(fēng)、無蟲害、無鼠害且溫度≤25℃、濕度≤60%的倉(cāng)庫(kù)內(nèi)貯存；不應(yīng)與有毒、有害、有異味、易揮發(fā)、易腐蝕的物品混裝運(yùn)輸或貯存。7保質(zhì)期在符合本標(biāo)準(zhǔn)的貯存條件下，凍干咖啡的保質(zhì)期宜為24個(gè)月。5T/CASME1712-2024附錄A（規(guī)范性附錄）凍干咖啡產(chǎn)品認(rèn)證檢驗(yàn)項(xiàng)目A.1表A.1規(guī)定了除4.2～4.6所列項(xiàng)目外，高品質(zhì)凍干咖啡產(chǎn)品認(rèn)證還應(yīng)檢驗(yàn)的項(xiàng)目。表A.1高品質(zhì)凍干咖啡產(chǎn)品認(rèn)證檢驗(yàn)項(xiàng)目1），234567896T/CASME1712-2024Generaltechnicalrequirementsforfreeze-driedcoffeeThisdocumentspecifiestheterminologyanddefinitions,,technicalrequirements,inspectionrules,labelingandmarking,packaging,transportation,storage,andshelflifeoffreeze-driedcoffee.Thisdocumentappliestotheproduction,inspection,andsaleoffreeze-driedcoffee.2NormativeReferencesThecontentsofthefollowingdocuments,throughnormativereferencesinthisdocument,constituteessentialprovisionsofthisdocument.Fordatedreferences,onlytheeditioncitedapplies.Forundatedreferences,thelatesteditionofthenormativedocument(includinganyamendments)applies.GB2760NationalFoodSafetyStandard-StandardsfortheUseofFoodAdditivesGB2761NationalFoodSafetyStandard-LimitsofMycotoxinsinFoodsGB2762NationalFoodSafetyStandard-LimitsofContaminantsinFoodsGB5009.3NationalFoodSafetyStandard-DeterminationofMoistureinFoodsGB5009.5NationalFoodSafetyStandard-DeterminationofProteininFoodsGB5009.11NationalFoodSafetyStandard-DeterminationofTotalArsenicandInorganicArsenicinFoodsGB5009.12NationalFoodSafetyStandard-DeterminationofLeadinFoodsGB5009.15NationalFoodSafetyStandard-DeterminationofCadmiuminFoodsGB/T5009.19—2008DeterminationofMultiresidueLevelsofOrganochlorinePesticidesinFoodsGB5009.22NationalFoodSafetyStandard-DeterminationofAflatoxinBandGinFoodsGB5009.96—2016NationalFoodSafetyStandard-DeterminationofOchratoxinAinFoodsGB5009.139NationalFoodSafetyStandard-DeterminationofCaffeineinBeveragesGB5413.29NationalFoodSafetyStandard-DeterminationofSolubilityinFoodsforInfantsandYoungChildrenandDairyProductsGB5749StandardsforDrinkingWaterQualityGB7101NationalFoodSafetyStandard-BeveragesGB7718—2011NationalFoodSafetyStandard-GeneralRulesfortheLabellingofPrepackagedFoodsGB/T15033GreenCoffee-OlfactoryandVisualExamination,andDeterminationofImpuritiesandDefectsGB/T23379—2009DeterminationofImidaclopridResiduesinFruits,Vegetables,andTea-High-PerformanceLiquidChromatography(HPLC)MethodT/CASME1712-2024GB28050—2011NationalFoodSafetyStandard-GeneralRulesforNutritionLabellingofPrepackagedFoodsNY/T604GreenCoffeeNY/T761—2008DeterminationofMulti-residuePesticidesofOrganophosphorus,Organochlorine,Pyrethroids,andCarbamatesinVegetablesandFruitsNY/T1680DeterminationofFourBenzimidazolePesticideResiduesIncludingCarbendaziminVegetablesandFruits-High-PerformanceLiquidChromatography(HPLC)MethodSN/T0519—2010MethodfortheDeterminationofPropiconazoleResiduesinImportedandExportedFoodsSN/T1952MethodfortheDeterminationofTebuconazoleResiduesinImportedandExportedCerealsandGrains-GasChromatography-MassSpectrometry(GC-MS)Method3TermsanddefinitionsThefollowingtermsanddefinitionsapplytothisdocument.3.1Freeze-driedcoffeeIrregularcrystallizedblock(particle)shapedinstantcoffeemadefromcoffeebeansasthemainrawmaterial,whichareroastedorunroasted,crushed,andthenextractedatlowtemperature.Thecoffeeextractisthenfrozenatlowtemperaturewithoutaddinganyfoodingredientsoradditives.Finally,itispreparedthroughultra-lowtemperaturevacuumfreeze-drying.3.2Modulatefreeze-driedcoffeeFreeze-driedcoffeethatisformulatedbyaddingrelevantfoodingredientsoradditives.4TechnicalRequirements4.1RequirementsforRawMaterialsandauxiliaryingredients4.1.1GreenCoffeeBeans:ShallcomplywiththeprovisionsofNY/T60Waterforproductionandprocessing:ShallcomplywiththeprovisionsofGB57Otherrawmaterialsandauxiliaryingredients:Shallcomplywiththecorrespondingstandardsandrelevantregulations,andnon-foodrawmaterialsandauxiliaryingredientsshallnotbeused.4.2Requirements4.2.1SensoryRequirementsShallcomplywiththeprovisionsofTable1.8T/CASME1712-2024Table1SensoryRequirementsItemRequirementTestMethodColorUniformcolorTake50gto100gofthesampleandplaceitinacleanwhiteporcelaincontainer.Observeitscolorandshapevisuallyunderdiffusedaylightorartificiallightsimilartodaylight.ShapeIrregularcrystallizedblock(particle)AromaandTasteHasthetypicalaromaoftheproduct,freefromabnormalodor,withgoodtasteandmouthfeelForeignImpurities,%(MassFraction)Freefromvisibleforeignimpurities4.2.2CharacteristicIndicatorsSolidfreeze-driedcoffeeproductsthathavenotbeendiluted(brewed)shouldmeettherequirementsofTable2.Table2CharacteristicIndicatorsItemIndicatorTestMethodCaffeine，mg/kg≥20000GB5009.139ThedilutedproductshouldmeettherequirementsofTable3accordingtothemixingratioormethodindicatedonthelabelTable3CharacteristicIndicatorsItemIndicatorTestMethodCaffeine，mg/kgGB5009.1394.2.3PhysicalandChemicalIndicatorsShallcomplywiththeprovisionsofTable4.Table4PhysicalandChemicalIndicatorsItemIndicatorTestMethodMoisture,g/100gSolubility,g/100gProtein,g/100g4.3MicrobialLimitShallcomplywiththeprovisionsofGB7101.4.4ContaminantLimitShallcomplywiththeprovisionsforsolidbeveragesinGB2762.4.5MycotoxinLimitT/CASME1712-2024ShallcomplywiththeprovisionsforsolidbeveragesinGB2761.4.6FoodAdditives4.6.1Nofoodadditivesshallbeaddedtofreeze-driedcoffee.4.6.2Thequalityoffoodadditivesusedinmodulatefreeze-driedcoffeeshouldcomplywiththecorrespondingfoodsafetystandardsandrelevantregulations,andtheuseoffoodadditivesshouldcomplywiththeprovisionsofGB2760.5InspectionRules5.1BatchFormationProductsprocessedwiththesamebatchofrawmaterials,ofthesameproducttype,inthesameshift,andwiththesamepackagingspecificationsshallbeconsideredasonebatch.5.2SamplingRandomlyselect6packagesfromthesamebatchofproducts.Dividethesamplesinto2portions,oneforinspectionandtheotherforbackup.5.3Inspection5.3.1FactoryInspectionEachbatchofproductsshallundergofactoryinspectionandcanonlybereleasedifitpassestheinspection.Theitemsforfactoryinspectionincludesensoryevaluation,moisturecontent,solubility,andnetcontent.5.3.2TypeInspectionUndernormalcircumstances,typeinspectionshouldbeconductedannually,coveringallitemsspecifiedinthisstandard.Itshouldalsobeconductedinanyofthefollowingsituations:a)Whentherearesignificantchangesinproductrawmaterials,formulas,orproductionprocesses;b)Whenproductionresumesafterbeinghaltedformorethanhalfayear;c)Whentherearesignificantdifferencesbetweentheresultsofthefactoryinspectionandtheprevioustypeinspection;d)Whenrequestedbythenationalsupervisoryandregulatoryauthorities.5.4JudgmentRules5.4.1Thebatchofproductsshallbejudgedasqualifiedifallinspectionresultscomplywiththerequirementsofthisstandard.5.4.2Ifanymicrobiologicalindicatorfailstomeettherequirementsofthisstandard,thebatchofproductsshallbejudgedasunqualified.5.4.3Ifanyitemotherthanmicrobiologicalindicatorsfailstomeettherequirementsofthisstandard,doublesamplingcanbeconductedforre-inspectionfromtheoriginalbatchofproducts.Thejudgmentshallbebasedontheresultsofthere-inspection.Ifanyindicatorfails,thebatchofproductsshallbejudgedasunqualified.T/CASME1712-20246Labeling,Packaging,Transportation,andStorage6.1Labeling6.1.1ThefoodlabelingforsalespackagingshallcomplywiththeprovisionsofGB7718andGB280Coffeeproductsthatmeettherequirementsofthisdocumentmaybelabeledas"Freeze-DriedCoffee."CoffeeproductsthatcomplywithAppendixAofthisdocument,uponcertification,maybelabeledas"High-QualityFreeze-DriedCoffee."ThelogoasshowninFigure1mayalsobeused.Figure1:Freeze-DriedCoffee6.2PackagingPackagingmaterialsandcontainersshouldcomplywiththecorrespondingfoodsafetystandardsandrelevantregulations.Thesealsshouldbetight,andthepackagingshouldbesecure.6.3TransportationandStorageTheproductshouldbeprotectedfromdirectsunlight,rain,andheavypressureduringtransportation;Theproductshouldbestoredinaclean,dark,dry,ventilated,pestfree,rodentfreewarehousewithatemperatureof≤25℃andhumidityof≤60%;Itshouldnotbetransportedorstoredtogetherwithtoxic,harmful,odorous,volatile,orcorrosivesubstances.7ShelfLifeUnderthestoragecondi