ICS

97.195；19.020

CCS

Y04

中華人民共和國(guó)國(guó)家標(biāo)準(zhǔn)

GB/T44202—2024

館藏絲織品老化程度測(cè)試樣品制備

Samplepreparationfortestingagingdegreeofsilktextileinmuseumcollections

2024-07-24發(fā)布2024-11-01實(shí)施

國(guó)家市場(chǎng)監(jiān)督管理總局發(fā)布

國(guó)家標(biāo)準(zhǔn)化管理委員會(huì)

GB/T44202—2024

目次

前言

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Ⅲ

1

范圍

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1

2

規(guī)范性引用文件

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1

3

術(shù)語和定義

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1

4

取樣

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1

4.1

取樣計(jì)劃

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4.2

取樣過程

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5

樣品處理

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2

5.1

樣品清洗

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2

5.2

樣品調(diào)濕

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2

6

樣品制備

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2

7

樣品信息登記

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2

附錄A（資料性）

館藏絲織品取樣信息記錄表樣式

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3

附錄B（資料性）

館藏絲織品老化程度測(cè)試樣品信息表樣式

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4

參考文獻(xiàn)

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5

Ⅰ

GB/T44202—2024

前言

本文件按照GB/T1.1—2020《標(biāo)準(zhǔn)化工作導(dǎo)則第1部分：標(biāo)準(zhǔn)化文件的結(jié)構(gòu)和起草規(guī)則》的規(guī)定

起草。

請(qǐng)注意本文件的某些內(nèi)容可能涉及專利。本文件的發(fā)布機(jī)構(gòu)不承擔(dān)識(shí)別專利的責(zé)任。

本文件由中華人民共和國(guó)國(guó)家文物局提出。

本文件由全國(guó)文物保護(hù)標(biāo)準(zhǔn)化技術(shù)委員會(huì)（SAC/TC289）歸口。

本文件起草單位：中國(guó)科學(xué)技術(shù)大學(xué)、中國(guó)國(guó)家博物館、福建理工大學(xué)、北京中科標(biāo)準(zhǔn)科技集團(tuán)有

限公司。

本文件主要起草人：龔鈺軒、龔德才、鐵付德、王志民、成維智、周光昭、喬成全、胡霜晴、

鐘博超、張曉寧、王開、羅賢娟。

Ⅲ

GB/T44202—2024

館藏絲織品老化程度測(cè)試樣品制備

1范圍

本文件規(guī)定了館藏絲織品老化程度測(cè)試樣品的取樣、處理、制備、樣品信息登記等要求。

本文件適用于館藏絲織品老化程度分析中氨基酸分析、掃描電子顯微鏡、熱重分析、傅里葉變換紅

外光譜、X射線粉末衍射測(cè)試方法的樣品制備。

2規(guī)范性引用文件

下列文件中的內(nèi)容通過文中的規(guī)范性引用而構(gòu)成本文件必不可少的條款。其中，注日期的引用文

件，僅該日期對(duì)應(yīng)的版本適用于本文件；不注日期的引用文件，其最新版本（包括所有的修改單）適用

于本文件。

GB/T6529—2008紡織品調(diào)濕和試驗(yàn)用標(biāo)準(zhǔn)大氣

GB/T13464—2008物質(zhì)熱穩(wěn)定性的熱分析試驗(yàn)方法

GB/T23863—2009博物館照明設(shè)計(jì)規(guī)范

GB/T32016—2015蠶絲氨基酸的測(cè)定

JGJ66—2015博物館建筑設(shè)計(jì)規(guī)范

3術(shù)語和定義

GB/T6529—2008界定的以及下列術(shù)語和定義適用于本文件。

3.1

絲織品老化程度agingdegreeofsilktextile

與新鮮蠶絲相比，館藏絲織品受損后所產(chǎn)生的微觀結(jié)構(gòu)和宏觀性能變化的水平。

4取樣

4.1取樣計(jì)劃

館藏絲織品老化程度測(cè)試樣品（以下簡(jiǎn)稱“樣品”，包括待測(cè)樣品和參比樣品1））制備應(yīng)與文物的

負(fù)責(zé)單位協(xié)商后根據(jù)取樣目的制定取樣計(jì)劃，取樣計(jì)劃的相關(guān)要求如下：

a）應(yīng)充分考慮歷次保護(hù)修復(fù)使用的材料和工藝對(duì)測(cè)試產(chǎn)生的影響；

b）根據(jù)需要和文物等級(jí)、保存狀況、病害、組織結(jié)構(gòu)等特點(diǎn)，確定取樣位置、取樣數(shù)量、取樣量

（如樣品尺寸、樣品面積和樣品質(zhì)量）、取樣方法、樣品包裝和保存方法等；

c）優(yōu)先從殘件（片）或?qū)ξ奈飪r(jià)值信息（如花紋、圖案等）影響較小的地方取樣；

d）確定樣品測(cè)試后剩余樣品的處置方式（如歸還原文物負(fù)責(zé)單位、自己留存等）。

4.2取樣過程